Evidence map›Paper›PMID 30934909›Full record

ArticleInternational journal of molecular sciences2019

Towards A New Approach for the Description of Cyclo⁻2,4-Dihydroxybenzoate, A Substance Which Effectively Mimics Zearalenone in Imprinted Polymers Designed for Analyzing Selected Mycotoxins in Urine.

Renata Gadzała-Kopciuch, Katarzyna Kwaśniewska, Agnieszka Ludwiczak, Piotr Skrzyniarz, Rafał Jakubowski, Wiesław Nowak, Andrzej Wojtczak, Bogusław Buszewski

Open access · goldAbstract read
In one paragraph

Article in International journal of molecular sciences, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
0.3field-weighted citation impact, top 27% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 4 citations in OpenAlex.

  1. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors at 1 institution in 1 country.

Renata Gadzała-KopciuchDepartment of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University in Torun, Gagarina 7, Pl-87 100 Toruń, Poland. rgadz@umk.pl.ORCID 0000-0002-1434-2824
Katarzyna KwaśniewskaDepartment of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University in Torun, Gagarina 7, Pl-87 100 Toruń, Poland. k.kwasniewska88@wp.pl.
Agnieszka LudwiczakDepartment of Geobotany and Landscape Planning, Faculty of Biology and Environmental Protection, Nicolaus Copernicus University in Torun, Lwowska 1, Pl-87 100 Toruń, Poland. agnieszka.b.1987@o2.pl.ORCID 0000-0003-1583-852X
Piotr SkrzyniarzInstitute of Physics, Faculty of Physics, Astronomy and Informatics, Nicolaus Copernicus University in Torun, Grudziądzka 5, 87⁻100 Toruń, Poland. piotr@skrzyniarz.com.pl.
Rafał JakubowskiInstitute of Physics, Faculty of Physics, Astronomy and Informatics, Nicolaus Copernicus University in Torun, Grudziądzka 5, 87⁻100 Toruń, Poland. rjakubowski@fizyka.umk.pl.ORCID 0000-0001-6837-5931
Wiesław NowakInterdisciplinary Center for Modern Technologies, Nicolaus Copernicus University in Torun, Wileńska 4, 87⁻100 Toruń, Poland. wiesiek@fizyka.umk.pl.ORCID 0000-0003-2584-1327
Andrzej WojtczakDepartment of Crystallochemistry and Biocrystalography, Faculty of Chemistry, Nicolaus Copernicus University in Torun, Gagarina 7, Pl-87 100 Toruń, Poland. awojt@chem.uni.torun.pl.ORCID 0000-0001-8801-7728
Bogusław BuszewskiDepartment of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University in Torun, Gagarina 7, Pl-87 100 Toruń, Poland. bbusz@umk.pl.
Nicolaus Copernicus University · PL

Funding

Narodowe Centrum Nauki PRELUDIUM 8 (2014/15/N/ST4/03723), PRELUDIUM 7 (2014/13/N/ST4/04119) and the MAESTRO project No. 2014/14/A/ST4/00641
6 · The paper itself

Abstract

A method of purifying cyclododecyl 2,4-dihydroxybenzoate as a potential replacement template molecule for preparation of molecularly-imprinted polymers for isolation of zearalenone in urine was developed. Full physicochemical characteristics of cyclododecyl 2,4-dihydroxybenzoate for the first time included crystallographic analysis and molecular modelling, which made possible the determination of the similarity between the cyclododecyl 2,4-dihydroxybenzoate and zearalenone molecules. The obtained molecularly-imprinted polymers show very high in vitro selectivity towards zearalenone due to specific interactions (e.g., hydrogen bonding, molecular recognition interaction). The achieved extraction recovery exceeds 94% at the tested concentration levels (20⁻500 ng·mL

Indexed as

Molecular ImprintingAdsorptionCalibrationCrystallography, X-RayCycloparaffinsDensity Functional TheoryHumansHydrogen BondingHydrogen-Ion ConcentrationHydroxybenzoatesKineticsLimit of DetectionMagnetic Resonance SpectroscopyMycotoxinsPolymersSpectroscopy, Fourier Transform InfraredCycloparaffinsHydroxybenzoatesMycotoxinsPolymersZearalenonecrystallographic analysismolecularly-imprinted polymersmolecularly imprinted solid-phase extraction (MISPE)molecular modelingzearalenone

Identifiers

PMID30934909
PMCPMC6479585
OpenAlexW2925101741

What OpenQuestion holds

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LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.