ArticleMikrochimica acta2019
Hybrid nanocomposites prepared from a metal-organic framework of type MOF-199(Cu) and graphene or fullerene as sorbents for dispersive solid phase extraction of polycyclic aromatic hydrocarbons.
Article in Mikrochimica acta, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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14 citing papers in PubMed, 104 citations in OpenAlex.
- Synthesis and application of polyoxometalate ionic liquid-coated ZnO nanoflowers for efficient extraction of tetracycline residues in food and environmental samples.RSC advances · 2026Article
- Cisplatin-loaded UiO-66-NHHeliyon · 2025Article
- An efficient deep eutectic magnetic nano gel for rapid ultrasound-assisted dispersive µ-solid phase extraction of residue of tetracyclines in food samples.Journal of food science and technology · 2023Article
- Carbon nanomaterial-based membranes in solid-phase extraction.Mikrochimica acta · 2023Review
- In-syringe solid-phase extraction of polycyclic aromatic hydrocarbons using an iron-carboxylate metal-organic framework and hypercrosslinked polymer composite gelatin cryogel-modified cellulose acetate adsorbent.Mikrochimica acta · 2022Article
- On the use of metal-organic frameworks for the extraction of organic compounds from environmental samples.Environmental science and pollution research international · 2021Review
- Efficient dispersive micro solid-phase extraction of antidepressant drugs by a robust molybdenum-based coordination polymer.Mikrochimica acta · 2021Article
- In-situ fabrication of zeolite imidazole framework@hydroxyapatite composite for dispersive solid-phase extraction of benzodiazepines and their determination with high-performance liquid chromatography-VWD detection.Mikrochimica acta · 2020Article
- Recent Advances in the Extraction of Polycyclic Aromatic Hydrocarbons from Environmental Samples.Molecules (Basel, Switzerland) · 2020Review
- In situ growth of metal-organic framework HKUST-1 in an organic polymer as sorbent for nitrated and oxygenated polycyclic aromatic hydrocarbon in environmental water samples prior to quantitation by HPLC-UV.Mikrochimica acta · 2020Article
- Molybdenum disulfide-hypercrosslinked polymer composite as an adsorbent for determination of polycyclic aromatic hydrocarbons in environmental water coupled with HPLC-FLD.Mikrochimica acta · 2020Article
- Graphene oxide/polydimethylsiloxane-coated stainless steel mesh for use in solid-phase extraction cartridges and extraction of polycyclic aromatic hydrocarbons.Mikrochimica acta · 2020Article
- Article
- A nanohybrid composed of polyoxotungstate and graphene oxide for dispersive micro solid-phase extraction of non-steroidal anti-inflammatory drugs prior to their quantitation by HPLC.Mikrochimica acta · 2019Article
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Authors and funding
3 authors at 2 institutions in 2 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Different types of hybrid nanocomposites were prepared from a copper-based metal-organic framework (MOF-199) and graphene (Gr) or fullerene (Fl). The porosity and quality of the nanocomposites were studied by scanning electron microscopy, transmission electron microscopy and BET surface area analysis. The nanocomposites are shown to be viable sorbents for the dispersive micro solid phase extraction of polycyclic aromatic hydrocarbons (PAHs) from environmental water samples. This is due to (a) the presence of MOF-199 which leads to improved adsorption capacity, and (b) the presence of Gr or Fl on the surface of MOF-199 which enhances the interaction with PAHs. Specifically, acenaphthene, anthracene, benz[a]anthracene, fluorene, naphthalene, 2-methylnaphthalene, and pyrene were studied. A comparison of the sorbents shows MOF-199/Gr to possess the highest adsorption affinity and to be most durable, probably a result of the high porosity of graphene. Following desorption with acetonitrile, the PAHs were quantified by GC with FID detection. Under the optimum conditions, limits of detection (at an S/N ratio of 3) range from 3 to 10 pg mL
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