Evidence map›Paper›PMID 30468072›Full record

ArticleThe Journal of organic chemistry2018

Photochemical Preparation of 1,2-Dihydro-3 H-indazol-3-ones in Aqueous Solvent at Room Temperature.

Jie S Zhu, Niklas Kraemer, Clarabella J Li, Makhluf J Haddadin, Mark J Kurth

Abstract read
In one paragraph

Article in The Journal of organic chemistry, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.

0numbers the graph read from it
0cells of the map it votes in
14citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

14 citing papers in PubMed.

  1. Article
  2. Article
  3. Review
  4. Article
  5. Article
  6. Electrochemical synthesis ofChemical science · 2022
    Article
  7. A photochemical C=C cleavage process: toward access to backboneBeilstein journal of organic chemistry · 2021
    Article
  8. Article
  9. Article
  10. Review
  11. Article
  12. Article
  13. Article
  14. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Jie S ZhuDepartment of Chemistry , University of California Davis , 1 Shields Avenue , Davis , California 95616 , United States.ORCID 0000-0003-3009-4135
Niklas KraemerDepartment of Chemistry , University of California Davis , 1 Shields Avenue , Davis , California 95616 , United States.
Clarabella J LiDepartment of Chemistry , University of California Davis , 1 Shields Avenue , Davis , California 95616 , United States.
Makhluf J HaddadinDepartment of Chemistry , American University of Beirut , Beirut , Lebanon.
Mark J KurthDepartment of Chemistry , University of California Davis , 1 Shields Avenue , Davis , California 95616 , United States.ORCID 0000-0001-8496-6125

Funding

SynthesisP30DK072517 · NIDDK · UNIVERSITY OF CALIFORNIA, SAN FRANCISCO · PI CIL, ONUR · 2005 to 2022
$18.1M
NIEHS Center for Health Effects of AgrochemicalsP30ES005707 · NIEHS · UNIVERSITY OF CALIFORNIA DAVIS · PI SCHENKER, MARC B · 1992 to 2006
$9.9M
XENOBIOTICS AND PRIMARY BILIARY CIRRHOSISR01DK067003 · NIDDK · UNIVERSITY OF CALIFORNIA DAVIS · PI GERSHWIN, MERRILL E · 2003 to 2017
$4.4M
MECHANISMS OF OXIDANT INDUCED LYMPHOCYTE REGULATIONF32ES005707 · NIEHS · WADSWORTH CENTER · PI KRIEGER, JIM A · 1995 to 1996
–
NIDDK NIH HHS P30 DK072517NIDDK NIH HHS R01 DK067003NIEHS NIH HHS F32 ES005707NIEHS NIH HHS P30 ES005707
6 · The paper itself

Abstract

o-Nitrosobenzaldehyde is a reactive intermediate useful in the synthesis of nitrogen heterocycles. Previous strategies for using o-nitrosobenzaldehyde involve its isolation via chromatography and/or formation under harsh conditions. Herein, this intermediate was photochemically generated in situ from o-nitrobenzyl alcohols in a mild, efficient manner for the construction of 1,2-dihydro-3 H-indazol-3-ones using an aqueous solvent at room temperature. This convenient reaction offers several advantages over reported methods. The commercially available photoreactor employed 3 × 18 W bulbs outputting broad emission above 365 nm.

Indexed as

Photochemical ProcessesTemperatureCatalysisIndazolesSolventsWaterIndazolesSolventsWater

Identifiers

PMID30468072
PMCPMC6467708

What OpenQuestion holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.