Evidence map›Paper›PMID 30255206›Full record

ArticleEnvironmental monitoring and assessment2018

Simultaneous determination of iprodione, procymidone, and chlorflurenol in lake water and wastewater matrices by GC-MS after multivariate optimization of binary dispersive liquid-liquid microextraction.

Nizamettin Özdoğan, Fatih Kapukıran, Gülşen Mutluoğlu, Dotse Selali Chormey, Sezgin Bakırdere

Abstract read
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In one paragraph

Article in Environmental monitoring and assessment, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
0.8field-weighted citation impact, top 31% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed, 15 citations in OpenAlex.

  1. Article
  2. Article
  3. Article
  4. Article
  5. Degradation of iprodione by a novel strainFrontiers in microbiology · 2022
    Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 2 institutions in 1 country.

Nizamettin ÖzdoğanDepartment of Environmental Engineer, Institute of Science, Bülent Ecevit University, 67100, Zonguldak, Turkey. nozdogan@beun.edu.tr.ORCID http://orcid.org/0000-0001-5520-5124
Fatih KapukıranDepartment of Environmental Engineer, Institute of Science, Bülent Ecevit University, 67100, Zonguldak, Turkey.
Gülşen MutluoğluFaculty of Art and Science, Department of Chemistry, Yıldız Technical University, 34210, Istanbul, Turkey.
Dotse Selali ChormeyFaculty of Art and Science, Department of Chemistry, Yıldız Technical University, 34210, Istanbul, Turkey.
Sezgin BakırdereFaculty of Art and Science, Department of Chemistry, Yıldız Technical University, 34210, Istanbul, Turkey.
Yıldız Technical University · TRBülent Ecevit University · TR

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This study reports the optimization of a binary dispersive liquid-liquid microextraction method for the determination of iprodione, procymidone, and chlorflurenol by gas chromatography mass spectrometry. The study was aimed at using two extraction solvents to increase the extraction efficiency of all analytes. The binary solvents recorded results higher than the mono-solvents. After examining the effects of main experimental parameters and their interactions by analysis of variance, 200 μL of binary mixture (dichloromethane and 1,2-dichloroethane), 2.5 mL of ethanol, and 15 s vortex were obtained as optimum parameters. The detection and quantification limits calculated for the analytes were found to be between 0.30-1.6 and 1.0-5.3 ng/mL, respectively. Enhancement in detection power calculated as a ratio of the binary extraction detection limit to the detection limit of direct GC-MS analysis was 105-, 214-, and 233-fold for chlorflurenol, iprodione, and procymidone, respectively. In order to check the accuracy of the developed method, recovery study was performed. Water sampled from a lake and two wastewater samples from treatment facilities were spiked at two concentrations, and the percent recovery calculated for the samples ranged between 87 and 116%. These results confirmed the suitability of the method to real samples for accurate determination of the analytes at trace levels.

Indexed as

Aminoimidazole CarboxamideBridged Bicyclo CompoundsEnvironmental MonitoringFluorenesGas Chromatography-Mass SpectrometryHydantoinsLakesLimit of DetectionLiquid Phase MicroextractionSolventsWastewaterWater Pollutants, ChemicalAminoimidazole CarboxamideBridged Bicyclo CompoundschlorflurenolFluorenesHydantoinsiprodioneprocymidoneSolventsWastewaterWater Pollutants, ChemicalBinary solvent extractionDLLMEExperimental designGC-MSPesticide

Identifiers

PMID30255206
OpenAlexW2893161926

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.