ArticleScience advances2018
Magic angle spinning spheres.
Article in Science advances, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 17 papers.
What it found
Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.
The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
The trial behind it
Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.
Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.
Who cites it
17 citing papers in PubMed.
- Single crystal sapphire spacers for in situ angle sensing and rotor stability diagnostics in MAS NMR.Solid state nuclear magnetic resonance · 2026Article
- Pseudo rotary resonance relaxation dispersion effects in isotropic samples.Magnetic resonance (Gottingen, Germany) · 2025Article
- High-field pulsed EPR spectroscopy under magic angle spinning.Science advances · 2024Article
- Automated test apparatus for bench-testing the magnetic field homogeneity of NMR transceiver coils.Journal of magnetic resonance open · 2024Article
- 3D-Printable centrifugal devices for biomolecular solid state NMR rotors.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2023Article
- Diamond rotors.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2023Article
- Ultrafast Magic Angle Spinning Solid-State NMR Spectroscopy: Advances in Methodology and Applications.Chemical reviews · 2023Review
- Cryogenic-compatible spherical rotors and stators for magic angle spinning dynamic nuclear polarization.Magnetic resonance (Gottingen, Germany) · 2023Article
- 3D-printed stators & drive caps for magic-angle spinning NMR.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2022Article
- Towards a native environment: structure and function of membrane proteins in lipid bilayers by NMR.Chemical science · 2021Review
- Reimagining magnetic resonance instrumentation using open maker tools and hardware as protocol.Journal of magnetic resonance open · 2021Article
- 3D printed sample tubes for solid-state NMR experiments.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2021Article
- Solid-state NMR spectroscopy.Nature reviews. Methods primers · 2021Article
- Residual dipolar line width in magic-angle spinning proton solid-state NMR.Magnetic resonance (Gottingen, Germany) · 2021Article
- High frequency dynamic nuclear polarization: New directions for the 21st century.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2019Review
- 3D-printed dissolvable inserts for efficient and customizable fabrication of NMR transceiver coils.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2019Article
- Additive fabrication for NMR probe builders.Progress in nuclear magnetic resonance spectroscopyReview
Corrections and comments
PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.
Authors and funding
11 authors.
Funding
Abstract
Magic angle spinning (MAS) is commonly used in nuclear magnetic resonance of solids to improve spectral resolution. Rather than using cylindrical rotors for MAS, we demonstrate that spherical rotors can be spun stably at the magic angle. Spherical rotors conserve valuable space in the probe head and simplify sample exchange and microwave coupling for dynamic nuclear polarization. In this current implementation of spherical rotors, a single gas stream provides bearing gas to reduce friction, drive propulsion to generate and maintain angular momentum, and variable temperature control for thermostating. Grooves are machined directly into zirconia spheres, thereby converting the rotor body into a robust turbine with high torque. We demonstrate that 9.5-mm-outside diameter spherical rotors can be spun at frequencies up to 4.6 kHz with N
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.