ArticleMagnetic resonance in chemistry : MRC2019
An NMR crystallography investigation of furosemide.
Article in Magnetic resonance in chemistry : MRC, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.
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Who cites it
5 citing papers in PubMed.
- Polymorph Identification for Flexible Molecules: Linear Regression Analysis of Experimental and Calculated Solution- and Solid-State NMR Data.The journal of physical chemistry. A · 2024Article
- Chemical Shift-Dependent Interaction Maps in Molecular Solids.Journal of the American Chemical Society · 2023Article
- Exploring the Potential of Multinuclear Solid-StateChemphyschem : a European journal of chemical physics and physical chemistry · 2023Article
- Combining X-ray and NMR Crystallography to Explore the Crystallographic Disorder in Salbutamol Oxalate.Crystal growth & design · 2022Article
- An NMR crystallography investigation of furosemide.Magnetic resonance in chemistry : MRC · 2019Article
Corrections and comments
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Authors and funding
3 authors.
Funding
Abstract
This paper presents an NMR crystallography study of three polymorphs of furosemide. Experimental magic-angle spinning (MAS) solid-state NMR spectra are reported for form I of furosemide, and these are assigned using density-functional theory (DFT)-based gauge-including projector augmented wave (GIPAW) calculations. Focusing on the three known polymorphs, we examine the changes to the NMR parameters due to crystal packing effects. We use a recently developed formalism to visualise which regions are responsible for the chemical shielding of particular sites and hence understand the variation in NMR parameters between the three polymorphs.
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