Evidence map›Paper›PMID 29963205›Full record

ArticleForensic toxicology2018

Differentiation of AB-FUBINACA and its five positional isomers using liquid chromatography-electrospray ionization-linear ion trap mass spectrometry and triple quadrupole mass spectrometry.

Takaya Murakami, Yoshiaki Iwamuro, Reiko Ishimaru, Satoshi Chinaka, Nariaki Takayama, Hiroshi Hasegawa

Open access · hybridAbstract read
In one paragraph

Article in Forensic toxicology, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
1.1field-weighted citation impact, top 28% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed, 16 citations in OpenAlex.

  1. Review
  2. Article
  3. Article
  4. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 2 institutions in 1 country.

Takaya Murakami1Forensic Science Laboratory, Ishikawa Prefectural Police H.Q., 1-1 Kuratsuki, Kanazawa, Ishikawa 920-8553 Japan.
Yoshiaki Iwamuro1Forensic Science Laboratory, Ishikawa Prefectural Police H.Q., 1-1 Kuratsuki, Kanazawa, Ishikawa 920-8553 Japan.
Reiko Ishimaru1Forensic Science Laboratory, Ishikawa Prefectural Police H.Q., 1-1 Kuratsuki, Kanazawa, Ishikawa 920-8553 Japan.
Satoshi Chinaka1Forensic Science Laboratory, Ishikawa Prefectural Police H.Q., 1-1 Kuratsuki, Kanazawa, Ishikawa 920-8553 Japan.
Nariaki Takayama1Forensic Science Laboratory, Ishikawa Prefectural Police H.Q., 1-1 Kuratsuki, Kanazawa, Ishikawa 920-8553 Japan.
Hiroshi Hasegawa2Institute of Science and Engineering, Kanazawa University, Kakuma, Kanazawa, Ishikawa 920-1192 Japan.
Ishikawa Prefectural Police · JPKanazawa University · JP

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

purposePositional isomer differentiation is crucial for forensic analysis. The aim of this study was to differentiate AB-FUBINACA positional isomers using liquid chromatography (LC)-electrospray ionization (ESI)-linear ion trap mass spectrometry (LIT-MS) and LC-ESI-triple quadrupole mass spectrometry (QqQ-MS).

methodsAB-FUBINACA, its two fluorine positional isomers on the phenyl ring, and three methyl positional isomers in the carboxamide side chain were analyzed by LC-ESI-LIT-MS and LC-ESI-QqQ-MS.

resultsFour of the positional isomers, excluding AB-FUBINACA and its 3-fluorobenzyl isomer, were chromatographically separated on an ODS column in isocratic mode. ESI-LIT-MS could discriminate only three isomers, i.e., the 2-fluorobenzyl isomer, the

conclusionsThe present LC-MS methodologies were useful for the differentiation of a series of AB-FUBINACA positional isomers.

Indexed as

AB-FUBINACAElectrospray ionizationLinear ion trap mass spectrometryLiquid chromatographyPositional isomer differentiationTriple quadrupole mass spectrometry

Identifiers

PMID29963205
PMCPMC6002426
OpenAlexW2792656176

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.