ArticleScientific reports2018
Microwave effects in the dilute acid hydrolysis of cellulose to 5-hydroxymethylfurfural.
Article in Scientific reports, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.
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Who cites it
8 citing papers in PubMed.
- Assessment of Different Niobium-Based Catalytic Systems for 5‑Hydroxymethylfurfural Production from Glucose and Microcrystalline Cellulose.ACS omega · 2026Article
- Cellulose from the banana stem: optimization of extraction by response surface methodology (RSM) and charaterization.Heliyon · 2022Article
- Microflow chemistry and its electrification for sustainable chemical manufacturing.Chemical science · 2022Review
- Conversion of bio-carbohydrates to 5-hydroxymethylfurfural in three-component deep eutectic solvent.RSC advances · 2022Article
- A Review of Microwave Synthesis of Zinc Oxide Nanomaterials: Reactants, Process Parameters and Morphoslogies.Nanomaterials (Basel, Switzerland) · 2020Review
- Catalytic Production of Levulinic Acid (LA) from Actual Biomass.Molecules (Basel, Switzerland) · 2019Review
- Eco-Friendly Ca-Montmorillonite Grafted by Non-Acidic Ionic Liquid Used as A Solid Acid Catalyst in Cellulose Hydrolysis to Reducing Sugars.Molecules (Basel, Switzerland) · 2019Article
- Recent Advances in the Microwave-Assisted Production of Hydroxymethylfurfural by Hydrolysis of Cellulose Derivatives-A Review.Molecules (Basel, Switzerland) · 2018Review
Corrections and comments
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Authors and funding
4 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
In this study, the effect of microwaves on the production of 5-hydroxymethylfurfural (HMF) in a biphasic system was evaluated via a kinetic analysis. The reaction system consisted of an acidified aqueous phase and methyl isobutyl ketone (MIBK) as an organic phase, in which HMF is extracted directly upon formation during the reaction. Two identically shaped reactors were used to assess the influence of microwaves on the production of HMF. A borosilicate glass reactor was used to heat the reaction mixture via microwaves directly, whereas the silicon carbide (SiC) wall of the second reactor absorbed all microwaves and hence the reactor content was heated via convective heat transfer. An identical temperature profile was imposed on both reactors. Cellulose, glucose and fructose were chosen as feedstocks for the conversion to HMF. It was observed that microwaves have a significant effect on the reactions. The hydrolysis of cellulose to glucose was a 2.3 folds faster in the presence of microwaves at the process conditions (0.046 M HCl, 177 °C). The isomerization of glucose to fructose showed a similar increase (factor 2.5). The required energy input for the reaction was systematically higher for the SiC reactor.
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Registered trials
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