ReviewAngewandte Chemie (International ed. in English)2018
Nanoscale Chemical Imaging of Zeolites Using Atom Probe Tomography.
Review in Angewandte Chemie (International ed. in English), 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 16 papers.
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Who cites it
16 citing papers in PubMed, 41 citations in OpenAlex.
- Multiscale spatiotemporal heterogeneity of zeolite-catalyzed methanol-to-hydrocarbons reaction.National science review · 2026Review
- 3D mapping of compositional gradients of core-shell structures in AgInNature communications · 2026Article
- Challenges and Opportunities in Core-Shell Zeolite Catalysts.ACS materials Au · 2026Review
- Self-formation of compositionally complex surface oxides on high entropy alloys observed by accelerated atom probe tomography: a route to sustainable catalysts.Materials horizons · 2024Article
- Elucidating the Structure and Composition of Individual Bimetallic Nanoparticles in Supported Catalysts by Atom Probe Tomography.Journal of the American Chemical Society · 2023Article
- Regulation of the Si/Al ratios and Al distributions of zeolites and their impact on properties.Chemical science · 2023Review
- Detecting Cage Crossing and Filling Clusters of Magnesium and Carbon Atoms in Zeolite SSZ-13 with Atom Probe Tomography.JACS Au · 2022Article
- Emerging analytical methods to characterize zeolite-based materials.National science review · 2022Review
- Nano-scale insights regarding coke formation in zeolite SSZ-13 subject to the methanol-to-hydrocarbons reaction.Catalysis science & technology · 2022Article
- Atom probe tomography.Nature reviews. Methods primers · 2021Article
- Acidity enhancement through synergy of penta- and tetra-coordinated aluminum species in amorphous silica networks.Nature communications · 2020Article
- Phase Segmentation in Atom-Probe Tomography Using Deep Learning-Based Edge Detection.Scientific reports · 2019Article
- Tracking the rearrangement of atomic configurations during the conversion ofChemical science · 2019Article
- Probing the Location and Speciation of Elements in Zeolites with Correlated Atom Probe Tomography and Scanning Transmission X-Ray Microscopy.ChemCatChem · 2019Article
- Nanoscale Chemical Imaging of Zeolites Using Atom Probe Tomography.Angewandte Chemie (International ed. in English) · 2018Review
- Isolating Clusters of Light Elements in Molecular Sieves with Atom Probe Tomography.Journal of the American Chemical Society · 2018Article
Corrections and comments
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Authors and funding
4 authors at 3 institutions in 2 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Understanding structure-composition-property relationships in zeolite-based materials is critical to engineering improved solid catalysts. However, this can be difficult to realize as even single zeolite crystals can exhibit heterogeneities spanning several orders of magnitude, with consequences for, for example, reactivity, diffusion as well as stability. Great progress has been made in characterizing these porous solids using tomographic techniques, though each method has an ultimate spatial resolution limitation. Atom probe tomography (APT) is the only technique so far capable of producing 3D compositional reconstructions with sub-nanometer-scale resolution, and has only recently been applied to zeolite-based catalysts. Herein, we discuss the use of APT to study zeolites, including the critical aspects of sample preparation, data collection, assignment of mass spectral peaks including the predominant CO peak, the limitations of spatial resolution for the recovery of crystallographic information, and proper data analysis. All sections are illustrated with examples from recent literature, as well as previously unpublished data and analyses to demonstrate practical strategies to overcome potential pitfalls in applying APT to zeolites, thereby highlighting new insights gained from the APT method.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.