Evidence map›Paper›PMID 29335163›Full record

ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2018

N,N-Diethylmethylamine as lineshape standard for NMR above 130 K.

Keith J Fritzsching, Boris Itin, Ann E McDermott

Open access · hybridAbstract read
In one paragraph

Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact, top 85% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 3 citations in OpenAlex.

  1. Resolution in cryogenic solid state NMR: Challenges and solutions.Protein science : a publication of the Protein Society · 2024
    Review
  2. Contribution of protein conformational heterogeneity to NMR lineshapes at cryogenic temperatures.Proceedings of the National Academy of Sciences of the United States of America · 2024
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors at 2 institutions in 1 country.

Keith J FritzschingDepartment of Chemistry, Columbia University, New York, NY 10027, United States.
Boris ItinNew York Structural Biology Center, New York, NY 10027, United States.
Ann E McDermottDepartment of Chemistry, Columbia University, New York, NY 10027, United States. Electronic address: aem5@columbia.edu.
Columbia University · USNew York Structural Biology Center · US

Funding

TR&D4: Integrated pipeline for data analysisP41GM118302 · NIGMS · NEW YORK STRUCTURAL BIOLOGY CENTER · PI PALMER, ARTHUR G · 2017 to 2021
$8.5M
Structural and Functional Studies of Potassium Channels by Solid State NMRR01GM088724 · NIGMS · COLUMBIA UNIV NEW YORK MORNINGSIDE · PI ANN E MCDERMOTT · 2009 to 2026
$5.6M
DYNAMIC NUCLEAR POLARIZATION SOLID STATE NMR SPECTROMETER FOR BIOMOLECULAR STUDIES10RR029249 · NCRR · NEW YORK STRUCTURAL BIOLOGY CENTER · PI MCDERMOTT, ANN E · 2010 to 2010
$2.3M
EXTRAMURAL RESEARCH FACILITIES CONSTRUCTIONC06RR015495 · NCRR · NEW YORK STRUCTURAL BIOLOGY CENTER · PI RIFKIND, RICHARD A · 2000 to 2000
$2.0M
NCRR NIH HHS C06 RR015495NCRR NIH HHS S10 RR029249NIGMS NIH HHS P41 GM118302NIGMS NIH HHS R01 GM088724
6 · The paper itself

Abstract

We demonstrate that N,N-Diethylmethylamine (DEMA) is a useful compound for shimming the magnetic field when doing NMR experiments at room temperature and 130 K, near the temperature used in many dynamic nuclear polarization (DNP) experiments. The resonance assigned to the N-methyl carbon in DEMA at 14.7 T and 140 K has a full-width-half-max linewidth of <4 Hz and has a spin-lattice relaxation time of 0.17 ± 0.03 s.

Indexed as

DiethylaminesMagnetic Resonance SpectroscopyPressureTemperatureDiethylaminesdiethylmethylamineDEMADNPDynamic nuclear polarizationN,N-DiethylmethylamineShimming

Identifiers

PMID29335163
PMCPMC5821130
OpenAlexW2776107274

What OpenQuestion holds

Textmetadata
LicenceCC BY-NC-ND
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.