ArticleOrganic letters2017
Synthesis of 1,2-Bis(trifluoromethylthio)arenes via Aryne Intermediates.
Article in Organic letters, 2017. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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Who cites it
4 citing papers in PubMed.
- Bromothiolation of Arynes for the Synthesis of 2-Bromobenzenethiol Equivalents.Organic letters · 2024Article
- Cascade trifluoromethylthiolation and cyclization ofBeilstein journal of organic chemistry · 2020Article
- 1,2-Bis(arylthio)arene synthesis via aryne intermediates.Chemical communications (Cambridge, England) · 2019Article
- Copper-mediated 1,2-bis(trifluoromethylation) of arynes.Chemical science · 2018Article
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2 authors.
Funding
Abstract
A general method for synthesis of 1,2-bis-trifluoromethylthioarenes has been developed. Arynes generated from silyl aryl triflates or halides react with bis(trifluoromethyl)disulfide to afford 1,2-bis-trifluoromethylthioarenes. Aryl, alkyl, ester, halide, and methoxy functionalities are compatible with reaction conditions. Use of bis(perfluoroaryl)disulfides gave moderate yields of aryne disulfenylation or cyclization to fluorinated dibenzothiophenes.
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