ArticleJournal of analytical methods in chemistry2016
Total Arsenic, Cadmium, and Lead Determination in Brazilian Rice Samples Using ICP-MS.
Article in Journal of analytical methods in chemistry, 2016. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.
What it found
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The trial behind it
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Who cites it
8 citing papers in PubMed, 56 citations in OpenAlex.
- Bioavailability and health risk assessment of potentially toxic elements in popcorn kernel from sandy loam Ferric Luvisol amended with municipal solid waste compost.Environmental geochemistry and health · 2022Trial
- Rapid and Accurate ED-XRF Quantification of Trace Arsenic in Rice-Based Foods Employing ANNs to Resolve Lead Spectral Interference.Foods (Basel, Switzerland) · 2026Article
- Specificity of Arsenic Stress Detection by Raman Spectroscopy During Co-Occurrences of Nitrogen Deficiency and Narrow Brown Leaf Spot.Analytical chemistry · 2026Article
- A novel approach for the identification of cadmium-chelating compounds in plant-based foods using SEC-ICP-MS/MS and SEC-QTOF-MS.Analytical and bioanalytical chemistry · 2025Article
- Quantitation of Arsenic in biological matrices: Use of Sector Field Inductively Coupled Plasma-Mass Spectrometry for Improved Accuracy and Specificity.Analytical letters · 2025Article
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- ICP-MS trace element analysis in serum and whole blood.PloS one · 2020Article
Corrections and comments
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Authors and funding
7 authors at 1 institution in 1 country.
Funding
No grant is acknowledged in the PubMed record.
Abstract
This study is aimed at investigating a suitable method for rice sample preparation as well as validating and applying the method for monitoring the concentration of total arsenic, cadmium, and lead in rice by using Inductively Coupled Plasma Mass Spectrometry (ICP-MS). Various rice sample preparation procedures were evaluated. The analytical method was validated by measuring several parameters including limit of detection (LOD), limit of quantification (LOQ), linearity, relative bias, and repeatability. Regarding the sample preparation, recoveries of spiked samples were within the acceptable range from 89.3 to 98.2% for muffle furnace, 94.2 to 103.3% for heating block, 81.0 to 115.0% for hot plate, and 92.8 to 108.2% for microwave. Validation parameters showed that the method fits for its purpose, being the total arsenic, cadmium, and lead within the Brazilian Legislation limits. The method was applied for analyzing 37 rice samples (including polished, brown, and parboiled), consumed by the Brazilian population. The total arsenic, cadmium, and lead contents were lower than the established legislative values, except for total arsenic in one brown rice sample. This study indicated the need to establish monitoring programs for emphasizing the study on this type of cereal, aiming at promoting the Public Health.
Identifiers
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.