ArticleAngewandte Chemie (International ed. in English)2016
Thermally Induced Silane Dehydrocoupling on Silicon Nanostructures.
Article in Angewandte Chemie (International ed. in English), 2016. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers.
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Who cites it
11 citing papers in PubMed.
- A fatty acid amide activates myeloid cells and improves neurovascular outcomes in retinal degeneration.Nature neuroscience · 2026Article
- Interferometric optical sensors based on porous silicon grafted with styrenic moieties for highly enhanced VOC detection.RSC advances · 2025Article
- Modification of Porous Silicon with an Amphiphilic Quaternary Ammonium Hydrocarbon for Nanomedicine Applications.Chemistry of materials : a publication of the American Chemical Society · 2025Article
- Intermediate Electronic Coupling via Silane and Germane Bridges in Silicon Quantum Dot-Molecular Hybrid Systems.Nano letters · 2025Article
- Designing Electrochemical Biosensing Platforms Using Layered Carbon-Stabilized Porous Silicon Nanostructures.ACS applied materials & interfaces · 2022Article
- Thermally Induced Silane Dehydrocoupling: Hydrophobic and Oleophilic Filter Paper Preparation for Water Separation and Removal from Organic Solvents.Materials (Basel, Switzerland) · 2021Article
- Systematic Degradation Rate Analysis of Surface-Functionalized Porous Silicon Nanoparticles.Materials (Basel, Switzerland) · 2019Article
- A Mini Review: Recent Advances in Surface Modification of Porous Silicon.Materials (Basel, Switzerland) · 2018Review
- A one-step method for covalent bond immobilization of biomolecules on silica operated in aqueous solution.Chemical science · 2018Article
- Enhanced Performance of a Molecular Photoacoustic Imaging Agent by Encapsulation in Mesoporous Silicon Nanoparticles.Advanced materials (Deerfield Beach, Fla.) · 2018Article
- Thermally Induced Silane Dehydrocoupling on Silicon Nanostructures.Angewandte Chemie (International ed. in English) · 2016Article
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Authors and funding
8 authors.
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Abstract
Organic trihydridosilanes can be grafted to hydrogen-terminated porous Si nanostructures with no catalyst. The reaction proceeds efficiently at 80 °C, and it shows little sensitivity to air or water impurities. The modified surfaces are stable to corrosive aqueous solutions and common organic solvents. Octadecylsilane H3 Si(CH2 )17 CH3 , and functional silanes H3 Si(CH2 )11 Br, H3 Si(CH2 )9 CH=CH2 , and H3 Si(CH2 )2 (CF2 )5 CF3 are readily grafted. When performed on a mesoporous Si wafer, the perfluoro reagent yields a superhydrophobic surface (contact angle 151°). The bromo-derivative is converted to azide, amine, or alkyne functional surfaces via standard transformations, and the utility of the method is demonstrated by loading of the antibiotic ciprofloxaxin (35 % by mass). When intrinsically photoluminescent porous Si films or nanoparticles are used, photoluminescence is retained in the grafted products, indicating that the chemistry does not introduce substantial nonradiative surface traps.
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