Evidence map›Paper›PMID 26924815›Full record

ArticleNanoscale research letters2016

Silica-Supported Titania-Zirconia Nanocomposites: Structural and Morphological Characteristics in Different Media.

Iryna Sulym, Olena Goncharuk, Dariusz Sternik, Ewa Skwarek, Anna Derylo-Marczewska, Wladyslaw Janusz, Vladimir M Gun'ko

Abstract read
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Article in Nanoscale research letters, 2016. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Efficient One-Pot Synthesis of TiOOxidative medicine and cellular longevity · 2022
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4 · The record

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PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Iryna SulymChuiko Institute of Surface Chemistry, NASU, 17 General Naumov Str., 03164, Kyiv, Ukraine.
Olena GoncharukChuiko Institute of Surface Chemistry, NASU, 17 General Naumov Str., 03164, Kyiv, Ukraine. iscgoncharuk@meta.ua.
Dariusz SternikFaculty of Chemistry, Maria Curie-Sklodowska University, 20-031, Lublin, Poland.
Ewa SkwarekFaculty of Chemistry, Maria Curie-Sklodowska University, 20-031, Lublin, Poland.
Anna Derylo-MarczewskaFaculty of Chemistry, Maria Curie-Sklodowska University, 20-031, Lublin, Poland.
Wladyslaw JanuszFaculty of Chemistry, Maria Curie-Sklodowska University, 20-031, Lublin, Poland.
Vladimir M Gun'koChuiko Institute of Surface Chemistry, NASU, 17 General Naumov Str., 03164, Kyiv, Ukraine.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A series of TiO2-ZrO2/SiO2 nanocomposites were synthesized using a liquid-phase method and characterized by various techniques, namely, nitrogen adsorption-desorption, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, high-resolution transmission electron microscopy, and photon correlation spectroscopy (PCS). It was revealed that the component ratio and calcination temperature affect the phase composition of nanocomposites. Composites TiZrSi1 (TiO2:ZrO2:SiO2 = 3:10:87) and TiZrSi2 (10:10:80) calcined at 1100 °С demonstrate the presence of t-ZrO2 crystallites in TiZrSi1 and ZrTiO4 phase in TiZrSi2. The samples calcined at 550 °С were amorphous as it was found from XRD data. According to the Raman spectra, the bands specific for anatase are observed in TiZrSi2. According to XPS data, Zr and Ti are in the highest oxidation state (+4). Textural analysis shows that initial silica is mainly meso/macroporous, but composites are mainly macroporous. The particle size distributions in aqueous media showed a tendency of increasing particle size with increasing TiO2 content in the composites.

Indexed as

NanocompositesNanocrystallinityParticle size distributionPhase compositionTiO2–ZrO2/SiO2

Identifiers

PMID26924815
PMCPMC4771666

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