Evidence map›Paper›PMID 26900260›Full record

ArticleSynlett : accounts and rapid communications in synthetic organic chemistry2015

Synthesis of Novel C-Pivot Lariat 18-Crown-6 Ethers and their Efficient Purification.

Susovan Jana, Vallabh Suresh, Salvatore D Lepore

Open access · greenAbstract read
In one paragraph

Article in Synlett : accounts and rapid communications in synthetic organic chemistry, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
0.3field-weighted citation impact, top 35% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 3 citations in OpenAlex.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors at 1 institution in 1 country.

Susovan JanaDepartment of Chemistry, Florida Atlantic University, 777 Glades Road, Boca Raton, Florida 33431, USA.
Vallabh SureshDepartment of Chemistry, Florida Atlantic University, 777 Glades Road, Boca Raton, Florida 33431, USA.
Salvatore D LeporeDepartment of Chemistry, Florida Atlantic University, 777 Glades Road, Boca Raton, Florida 33431, USA.
Florida Atlantic University · US

Funding

Synthesis of a Bridged Bicyclic Natural Product Using Allenyl EstersR15GM110651 · NIGMS · FLORIDA ATLANTIC UNIVERSITY · PI LEPORE, SALVATORE D · 2014 to 2020
$1.2M
NIGMS NIH HHS R15 GM110651
6 · The paper itself

Abstract

The syntheses of various lariat ethers including several not previously reported and their efficient purification are presented. The synthesis route brings together reactions from a variety of previous works leading to a robust and generalized approach to these C-pivot lariats. The main steps are condensation of functionalized diols with pentaethylene glycol ditosylate in the presence of potassium as a templating cation. Purification of the final products was achieved without chromatography by extracting from an aqueous potassium hydroxide solution.

Indexed as

18-crown-6C-pivot lariat etherscrown compoundsmacrocylespotassium hydroxide purification

Identifiers

PMID26900260
PMCPMC4756917
OpenAlexW2462604119

What OpenQuestion holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.