ArticleActa crystallographica. Section E, Crystallographic communications2015
Crystal structure of tris-(μ-bis-{4-[(pyridin-2-yl-methyl-idene)amino]-phen-yl}methane-κ(4) N,N':N'',N''')dizinc tetra-kis-(tetra-fluorido-borate) aceto-nitrile tris-olvate.
Article in Acta crystallographica. Section E, Crystallographic communications, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The asymmetric unit of the title compound, [Zn2(C25H20N4)3](BF4)4·3CH3CN, consists of one dinuclear Zn(II) complex cation with a triple-helical [Zn2 L 3](4+) motif (L is bis-{4-[(pyridin-2-yl-methyl-idene)amino]-phen-yl}methane), four BF4 (-) anions and three CH3CN solvent mol-ecules. The Zn⋯Zn separation is 11.3893 (14) Å and the ligands wrap around the two Zn(II) atoms, forming a triple helix as defined by the Zn-N-N-Zn torsion angles of 104.05 (18), 99.06 (19) and 101.40 (19)°. The Zn-N(pyrid-yl) distances in the octahedral ZnN6 coordination sphere are in the range 2.128 (5)-2.190 (5) Å and the Zn-N(imine) distances are in the range 2.157 (5)-2.277 (5) Å.
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