Evidence map›Paper›PMID 26791345›Full record

ArticleJournal of chromatographic science

Fingerprint Analysis of Desmodium Triquetrum L. Based on Ultra Performance Liquid Chromatography with Photodiode Array Detector Combined with Chemometrics Methods.

Meiling Zhang, Cui Zhao, Xianrui Liang, Yin Ying, Bing Han, Bo Yang, Cheng Jiang

Abstract readValidation Study
In one paragraph

Article in Journal of chromatographic science. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Meiling ZhangDepartment of Pharmacy, Tongde Hospital of Zhejiang Province, 234 Gucui Road, Hangzhou 310012, China zml9998@sina.com.
Cui ZhaoKey Laboratory for Green Pharmaceutical Technologies and Related Equipment of Ministry of Education, Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou 310014, China.
Xianrui LiangKey Laboratory for Green Pharmaceutical Technologies and Related Equipment of Ministry of Education, Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou 310014, China.
Yin YingDepartment of Pharmacy, Tongde Hospital of Zhejiang Province, 234 Gucui Road, Hangzhou 310012, China.
Bing HanDepartment of Pharmacy, Tongde Hospital of Zhejiang Province, 234 Gucui Road, Hangzhou 310012, China.
Bo YangDepartment of Pharmacy, Tongde Hospital of Zhejiang Province, 234 Gucui Road, Hangzhou 310012, China.
Cheng JiangDepartment of Pharmacy, Tongde Hospital of Zhejiang Province, 234 Gucui Road, Hangzhou 310012, China.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A fingerprinting approach was developed by means of ultra high-performance liquid chromatography with photodiode array detector for the quality control of Desmodium triquetrum L., an herbal medicine widely used for clinical purposes. Ten batches of raw material samples of D. triquetrum were collected from different regions of China. All UPLC analyses were carried out on a Waters ACQUITY UPLC BEH shield RP18 column (2.1 × 50 mm, 1.7 µm particle size) at 60°C, with a gradient mobile phase composed of 0.1% aqueous formic acid and acetonitrile at a flow rate of 0.45 mL/min. The method validation results demonstrated the developed method possessing desirable reproducibility, efficiency, and allowing fingerprint analysis in one chromatographic run within 13 min. The quality assessment was achieved by using chemometrics methods including similarity analysis, hierarchical clustering analysis and principal component analysis. The developed method can be used for further quality control of D. triquetrum.

Indexed as

Chromatography, LiquidCluster AnalysisFabaceaeLimit of DetectionPrincipal Component AnalysisReference StandardsReproducibility of ResultsSpectrophotometry, Ultraviolet

Identifiers

PMID26791345
PMCPMC4890440

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.