ArticleJournal of colloid and interface science2015
Insights into the synthesis of layered double hydroxide (LDH) nanoparticles: Part 1. Optimization and controlled synthesis of chloride-intercalated LDH.
Article in Journal of colloid and interface science, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 13 papers.
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13 citing papers in PubMed, 69 citations in OpenAlex.
- From Coprecipitation to Nanostructure: Formation, Morphology, and Reactive-Site Accessibility in Fe-Containing Binary Layered Double Hydroxides.Nanomaterials (Basel, Switzerland) · 2026Review
- Article
- Supersaturation-controlled morphology and phase evolution of NiCo LDH in controllable and continuous flow synthesis.PloS one · 2025Article
- Synthesis of layered double hydroxides: Investigating the impact of stirring conditions and reactor design parameters.Heliyon · 2024Article
- Nanoengineered injectable hydrogels derived from layered double hydroxides and alginate for sustained release of protein therapeutics in tissue engineering applications.Journal of nanobiotechnology · 2023Article
- Layered Double Hydroxides for Regulating Phosphate in Water to Achieve Long-Term Nutritional Management.ACS omega · 2023Review
- Formation Optimization, Characterization and Antioxidant Activity of Auricularia auricula-judae Polysaccharide Nanoparticles Obtained via Antisolvent PrecipitationMolecules (Basel, Switzerland) · 2022Article
- Tailored Adhesion Properties of Acrylate Adhesives on Al Alloys by the Addition of Mn-Al-LDH.Polymers · 2021Article
- Graphene and other 2D materials: a multidisciplinary analysis to uncover the hidden potential as cancer theranostics.Theranostics · 2020Review
- Formation of high crystalline LDH sludge for removing Cu and Zn from wastewater by controlled double-jet precipitation.Environmental science and pollution research international · 2019Article
- Article
- Hydrodynamic assembly of two-dimensional layered double hydroxide nanostructures.Nature communications · 2018Article
- Gadolinium-based layered double hydroxide and graphene oxide nano-carriers for magnetic resonance imaging and drug delivery.Chemistry Central journal · 2017Review
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Authors and funding
3 authors at 1 institution in 1 country.
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Abstract
Layered double hydroxide (LDH) nanoparticles have excellent anion-intercalating property, and their potential as theranostic nanovectors is high. However, understanding of the control of the mean particle size (MPS) and achievement of monodispersed particle size distribution (PSD) remains elusive. Herein, with the aid of statistical design of experiments on a model system of Cl(-)-intercalated (Zn, Al)-LDH, controlled synthesis of single crystalline nanoparticles using the coprecipitation method followed by hydrothermal treatment (HT) was achieved in three steps. First, a 2(4-1) design enabled the identification of influential parameters for MPS (i.e., salt concentration, molar ratio of carbonate to aluminum, solution addition rate, and interaction between salt concentration and stirring rate) and PSD (i.e., salt concentration and stirring rate), as well as the optimum coprecipitation conditions that result in a monodispersed PSD (i.e., low salt concentration and high stirring rate). Second, a preliminary explanation of the HT was suggested and the optimum HT conditions for obtaining ideal Gaussian PSD with chi-squared (χ(2))<3 were found to be 85°C for 5 h. Third, using a central composite design, a quantitative MPS model, expressed in terms of the significant factors, was developed and experimentally verified to synthesize nearly monodispersed LDH nanoparticles with MPS ∼200-500 nm.
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