Evidence map›Paper›PMID 26090187›Full record

ArticleActa crystallographica. Section E, Crystallographic communications2015

Redetermined crystal structure of β-dl-me-thio-nine at 320 K.

Carl Henrik Görbitz, Jan Christian Paulsen, Jon Borgersen

Abstract read
In one paragraph

Article in Acta crystallographica. Section E, Crystallographic communications, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.

0numbers the graph read from it
0cells of the map it votes in
5citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

5 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors.

Carl Henrik GörbitzDepartment of Chemistry, University of Oslo, PO Box 1033 Blindern, N-0315 Oslo, Norway.
Jan Christian PaulsenDepartment of Chemistry, University of Oslo, PO Box 1033 Blindern, N-0315 Oslo, Norway.
Jon BorgersenDepartment of Physics, University of Oslo, PO Box 1048 Blindern, N-0316 Oslo, Norway.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The structure of β-dl-me-thio-nine, C5H11NO2S, in the space group C2/c, is here confirmed to be fully ordered all the way up to the phase transition at approximately 326 K, where displacive sliding of mol-ecular bilayers gives the disordered P21/c α form [data at 340 K; Görbitz (2014). Acta Cryst. E70, 341-343]. The geometry of hydrogen bonds in LD-LD hydrogen-bonding patterns [Görbitz et al. (2009). Acta Cryst. B65, 393-400] at the hydro-philic core of each mol-ecular bilayer are virtually unperturbed by the phase shift, but the C-C-S-C torsion angle of the side chain changes from trans at 320 K to gauche+ for the major conformation at 340 K.

Indexed as

amino acidcrystal structuredisorderphase transition

Identifiers

PMID26090187
PMCPMC4459326

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.