ArticleActa crystallographica. Section E, Crystallographic communications2015
Crystal structure of [bis-(2,6-diiso-propyl-phen-yl) phosphato-κO]tris-(methanol-κO)lithium methanol monosolvate.
Article in Acta crystallographica. Section E, Crystallographic communications, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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Who cites it
4 citing papers in PubMed.
- Diarylphosphate as a New Route for Design of Highly Luminescent Ln Complexes.Molecules (Basel, Switzerland) · 2020Article
- Crystal structure of tris-[bis-(2,6-diiso-propyl-phen-yl) phosphato-κActa crystallographica. Section E, Crystallographic communications · 2019Article
- Bis[μ-bis-(2,6-diiso-propyl-phen-yl) phosphato-κActa crystallographica. Section E, Crystallographic communications · 2019Article
- [Bis(2,6-diiso-propyl-phen-yl) phosphato-κActa crystallographica. Section E, Crystallographic communications · 2018Article
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5 authors.
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Abstract
Crystals of the title compound, [Li{OOP(O-2,6-(i)Pr2C6H3)2}(CH3OH)3]·CH3OH or [Li(C24H34O4P)(CH3OH)3]·CH3OH, have been formed in the reaction between HOOP(O-2,6-(i)Pr2C6H3)2 and LiOH in methanol. The title compound is of inter-est as it represents the first reported crystal structure of the family of lithium phosphate diesters. The {Li(CH3OH)3[O2P(O-(i)Pr2C6H3)2]} unit displays the Li atom in a slightly distorted tetra-hedral coordination environment and exhibits one intra-molecular O-H⋯O hydrogen bond between a coordinating methanol mol-ecule and the terminal non-coordinating O atom of the phosphate group. The unit is connected with two non-coordinating methanol mol-ecules through two inter-molecular O-H⋯O hydrogen bonds, and with a neighbouring unit through two other O-H⋯O inter-actions. These inter-molecular hydrogen bonds lead to the formation of infinite chains along [100]. There are no significant inter-actions between the chains.
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