Evidence map›Paper›PMID 25878867›Full record

ArticleActa crystallographica. Section E, Crystallographic communications2015

Crystal structure of 2-[4-(4-chloro-phen-yl)-1-(4-meth-oxy-phen-yl)-2-oxoazetidin-3-yl]benzo[de]iso-quinoline-1,3-dione dimethyl sulfoxide monosolvate.

Ísmail Çelik, Mehmet Akkurt, Aliasghar Jarrahpour, Javad Ameri Rad, Ömer Çelik

Abstract read
In one paragraph

Article in Acta crystallographica. Section E, Crystallographic communications, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Ísmail ÇelikDepartment of Physics, Faculty of Arts and Sciences, Cumhuriyet University, 06532 Sivas, Turkey.
Mehmet AkkurtDepartment of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.
Aliasghar JarrahpourDepartment of Chemistry, College of Sciences, Shiraz University, 71454 Shiraz, Iran.
Javad Ameri RadDepartment of Chemistry, College of Sciences, Shiraz University, 71454 Shiraz, Iran.
Ömer ÇelikDepartment of Physics, Faculty of Education, Dicle University, 21280, Diyarbakir, Turkey ; Science and Technology Application and Research Center, Dicle University, 21280, Diyarbakir, Turkey.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

In the title solvated compound, C28H19N2O4·C2H6OS, the central β-lactam ring is almost planar (r.m.s. deviation = 0.002 Å). It makes dihedral angles of 1.92 (11), 83.23 (12) and 74.90 (10)° with the meth-oxy- and chloro-phenyl rings and the ring plane of the 1H-benzo[de]iso-quinoline-1,3(2H)-dione group [maximum deviation = 0.089 (1)], respectively. An intra-molecular C-H⋯O hydrogen bond closes an S(6) ring and helps to establish the near coplanarity of the β-lactam and meth-oxy-benzene rings. In the crystal, the components are linked by C-H⋯O hydrogen bonds, C-H⋯π inter-actions and aromatic π-π stacking inter-actions [centroid-to-centroid distances = 3.6166 (10) and 3.7159 (10) Å], resulting in a three-dimensional network, The dimethyl sulfoxide solvent mol-ecule is disordered over two sets of sites in a 0.847 (2):0.153 (2) ratio.

Indexed as

1H-benzo[de]iso­quinoline-1,3(2H)-dione groupazetidin-2-onescrystal structuredisorderβ-lactam ring

Identifiers

PMID25878867
PMCPMC4384601

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.