Evidence map›Paper›PMID 25649027›Full record

ArticleNanotechnology2015

Electrochemical annealing of nanoporous gold by application of cyclic potential sweeps.

Abeera Sharma, Jay K Bhattarai, Allan J Alla, Alexei V Demchenko, Keith J Stine

Abstract read
In one paragraph

Article in Nanotechnology, 2015. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 10 papers.

0numbers the graph read from it
0cells of the map it votes in
10citing papers in PubMed
2.2field-weighted citation impact, top 12% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

10 citing papers in PubMed, 28 citations in OpenAlex.

  1. Review
  2. Facile fabrication of hierarchically nanostructured gold electrode for bio-electrochemical applications.Journal of electroanalytical chemistry (Lausanne, Switzerland) · 2022
    Article
  3. Article
  4. Article
  5. Article
  6. Review
  7. Review
  8. Article
  9. Article
  10. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 1 institution in 1 country.

Abeera SharmaCenter for Nanoscience, Department of Chemistry and Biochemistry, University of Missouri-Saint Louis, Saint Louis, MO 63121, USA.
Jay K BhattaraiCenter for Nanoscience, Department of Chemistry and Biochemistry, University of Missouri-Saint Louis, Saint Louis, MO 63121, USA.
Allan J AllaCenter for Nanoscience, Department of Chemistry and Biochemistry, University of Missouri-Saint Louis, Saint Louis, MO 63121, USA.
Alexei V DemchenkoDepartment of Chemistry and Biochemistry, University of Missouri-Saint Louis, Saint Louis, MO 63121, USA.
Keith J StineCenter for Nanoscience, Department of Chemistry and Biochemistry, University of Missouri-Saint Louis, Saint Louis, MO 63121, USA.
University of Missouri–St. Louis · US

Funding

Automation of the chemical synthesis of human milk oligosaccharidesR01GM111835 · NIGMS · SAINT LOUIS UNIVERSITY · PI DEMCHENKO, ALEXEI V · 2014 to 2023
$2.5M
Development and Application of Surface-Tethered Iterative Carbohydrate SynthesisR01GM090254 · NIGMS · UNIVERSITY OF MISSOURI-ST. LOUIS · PI STINE, KEITH J. · 2009 to 2012
$1.1M
NIGMS NIH HHS R01 GM090254NIGMS NIH HHS R01-GM090254NIGMS NIH HHS R01 GM111835NIGMS NIH HHS R01-GM111835
6 · The paper itself

Abstract

An electrochemical method for annealing the pore sizes of nanoporous gold (NPG) is reported. The pore sizes of NPG can be increased by electrochemical cycling with the upper potential limit being just at the onset of gold oxide formation. This study has been performed in electrolyte solutions including potassium chloride, sodium nitrate and sodium perchlorate. Scanning electron microscopy images have been used for ligament and pore size analysis. We examine the modifications of NPG due to annealing using electrochemical impedance spectroscopy, and cyclic voltammetry and offer a comparison of the surface coverage using the gold oxide stripping method as well as the method in which electrochemically accessible surface area is determined by using a diffusing redox probe. The effect of additives adsorbed on the NPG surface when subjected to annealing in different electrolytes as well as the subsequent structural changes in NPG are also reported. The effect of the annealing process on the application of NPG as a substrate for glucose electro-oxidation is briefly examined.

Indexed as

Biosensing TechniquesDielectric SpectroscopyGlucoseGoldMetal NanoparticlesMicroscopy, Electron, ScanningPorosityGlucoseGold

Identifiers

PMID25649027
PMCPMC4350776
OpenAlexW1969012895

What OpenQuestion holds

Textmetadata
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Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.