ArticleActa crystallographica. Section E, Structure reports online2014
Crystal structure of 1-(4-formyl-benzyl-idene)thio-semicarbazone.
Article in Acta crystallographica. Section E, Structure reports online, 2014. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
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Who cites it
3 citing papers in PubMed.
- Synthesis, crystal structure and Hirshfeld surface analysis of 4-{(1Acta crystallographica. Section E, Crystallographic communications · 2024Article
- Crystal structure of 4-[(E)-(2-carbamo-thio-ylhydrazinyl-idene)meth-yl]benzoic acid.Acta crystallographica. Section E, Crystallographic communications · 2015Article
- Crystal structures of crotonaldehyde semicarbazone and crotonaldehyde thiosemicarbazone from X-ray powder diffraction data.Acta crystallographica. Section E, Crystallographic communications · 2015Article
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Authors and funding
3 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
The asymmetric unit of the title compound, C9H9N3OS, contains two approximately planar mol-ecules (r.m.s. deviations for 14 non-H atoms = 0.094 and 0.045 Å), with different conformations. In one of them, the C=O group is syn to the S atom and in the other it is anti. Each mol-ecule features an intra-molecular N-H⋯N hydrogen bond, which generates an S(5) ring. In the crystal, mol-ecules are linked by N-H⋯O and N-H⋯S hydrogen bonds, generating discrete networks; the syn mol-ecules form [010] chains and the anti mol-ecules form (100) sheets.
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Registered trials
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