Evidence map›Paper›PMID 25309199›Full record

ArticleActa crystallographica. Section E, Structure reports online2014

Crystal structure of 4-[(E)-(4-chloro-benzyl-idene)amino]-3-(2-methyl-benz-yl)-1H-1,2,4-triazole-5(4H)-thione.

Kamni, B K Sarojini, P S Manjula, B Narayana, Sumati Anthal, Rajni Kant

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Article in Acta crystallographica. Section E, Structure reports online, 2014. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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4 · The record

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5 · Who and what money

Authors and funding

6 authors.

KamniSchool of Physics, Shri Mata Vaishno Devi University, Katra 182 320, J&K, India.
B K SarojiniDepartment of Chemistry, Mangalore University, Mangalagangotri 574 199, D.K., Mangalore, India.
P S ManjulaDepartment of Chemistry, P A College of Engineering, Nadupadavu 574 153, D.K., Mangalore, India.
B NarayanaDepartment of Chemistry, Mangalore University, Mangalagangotri 574 199, D.K., Mangalore, India.
Sumati AnthalX-ray Crystallography Laboratory, Post-Graduate Department of Physics & Electronics, University of Jammu, Jammu Tawi 180 006, India.
Rajni KantX-ray Crystallography Laboratory, Post-Graduate Department of Physics & Electronics, University of Jammu, Jammu Tawi 180 006, India.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

In the title mol-ecule, C17H15ClN4S, the benzene rings form dihedral angles of 16.6 (1) and 77.2 (1)° with the triazole ring. The dihedral angle between the benzene rings is 86.6 (1)°. In the crystal, pairs of N-H⋯S hydrogen bonds form inversion dimers with graph-set notation R 2 (2)(8). Weak C-H⋯S hydrogen bonds link these dimers into layers parallel to (100). Weak intra-molecular C-H⋯S and C-H⋯N contacts are observed.

Indexed as

1,2,4-triazolecrystal structurehydrogen bondingSchiff base

Identifiers

PMID25309199
PMCPMC4186062

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