ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2014
Accurate scoring of non-uniform sampling schemes for quantitative NMR.
Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2014. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 33 papers.
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Who cites it
33 citing papers in PubMed.
- Decoherence Principles and Algorithms for One-Dimensional Nonuniform Sampling Schedules for Multidimensional NMR.Analytical chemistry · 2025Article
- Non-Uniform Sampling for Quantitative NOESY.Magnetic resonance in chemistry : MRC · 2025Article
- Evaluating metrics of spectral quality in nonuniform sampling.Journal of magnetic resonance open · 2025Article
- Ultrafast Nuclear Magnetic Resonance as a Tool to Detect Rapid Chemical Change in Solution.ACS physical chemistry Au · 2024Review
- Conformational Dynamics of an Amyloidogenic Intermediate of Transthyretin: Implications for Structural Remodeling and Amyloid Formation.Journal of molecular biology · 2024Article
- nus-tool: A unified program for generating and analyzing sample schedules for nonuniformly sampled NMR experiments.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2023Article
- NMR methods for the analysis of mixtures.Chemical communications (Cambridge, England) · 2022Review
- High fidelity sampling schedules for NMR spectra of high dynamic range.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2022Article
- Clustered sparsity and Poisson-gap sampling.Journal of biomolecular NMR · 2021Article
- Role of Active Site Loop Dynamics in Mediating Ligand Release fromBiochemistry · 2021Article
- Reducing the measurement time of exact NOEs by non-uniform sampling.Journal of biomolecular NMR · 2020Article
- Non-Uniform Sampling in NMR Spectroscopy and the Preservation of Spectral Knowledge in the Time and Frequency Domains.The journal of physical chemistry. A · 2020Article
- The influence of the probability density function on spectral quality in nonuniformly sampled multidimensional NMR.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2020Article
- A Dynamic Switch in Inactive p38γ Leads to an Excited State on the Pathway to an Active Kinase.Biochemistry · 2019Article
- Extreme Nonuniform Sampling for Protein NMR Dynamics Studies in Minimal Time.Journal of the American Chemical Society · 2019Article
- Article
- Assessing the potential of quantitative 2D HSQC NMR inJournal of biomolecular NMR · 2019Article
- NMR Measurements Reveal the Structural Basis of Transthyretin Destabilization by Pathogenic Mutations.Biochemistry · 2018Article
- CH···O Hydrogen Bonds Mediate Highly Specific Recognition of Methylated CpG Sites by the Zinc Finger Protein Kaiso.Biochemistry · 2018Article
- Slow Dynamics of Tryptophan-Water Networks in Proteins.Journal of the American Chemical Society · 2018Article
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4 authors.
Funding
Abstract
Non-uniform sampling (NUS) in NMR spectroscopy is a recognized and powerful tool to minimize acquisition time. Recent advances in reconstruction methodologies are paving the way for the use of NUS in quantitative applications, where accurate measurement of peak intensities is crucial. The presence or absence of NUS artifacts in reconstructed spectra ultimately determines the success of NUS in quantitative NMR. The quality of reconstructed spectra from NUS acquired data is dependent upon the quality of the sampling scheme. Here we demonstrate that the best performing sampling schemes make up a very small percentage of the total randomly generated schemes. A scoring method is found to accurately predict the quantitative similarity between reconstructed NUS spectra and those of fully sampled spectra. We present an easy-to-use protocol to batch generate and rank optimal Poisson-gap NUS schedules for use with 2D NMR with minimized noise and accurate signal reproduction, without the need for the creation of synthetic spectra.
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