ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2012
A comparison of NCO and NCA transfer methods for biological solid-state NMR spectroscopy.
Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2012. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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Who cites it
14 citing papers in PubMed.
- Optimal control of spin systems.Science advances · 2026Review
- Dipolar Recoupling in Rotating Solids.Chemical reviews · 2024Review
- High-efficiency low-powerJournal of magnetic resonance (San Diego, Calif. : 1997) · 2024Article
- Assignment of aromatic side-chain spins and characterization of their distance restraints at fast MAS.Journal of structural biology: X · 2023Article
- Maximizing efficiency of dipolar recoupling in solid-state NMR using optimal control sequences.Science advances · 2021Article
- Characterization of the Conjugation Pattern in Large Polysaccharide-Protein Conjugates by NMR Spectroscopy.Angewandte Chemie (International ed. in English) · 2017Article
- Solid state NMR chemical shift assignment and conformational analysis of a cellulose binding protein facilitated by optimized glycerol enrichment.Journal of biomolecular NMR · 2014Article
- Solid-state NMR studies of metal-free SOD1 fibrillar structures.Journal of biological inorganic chemistry : JBIC : a publication of the Society of Biological Inorganic Chemistry · 2014Article
- Dipolar Assisted Assignment Protocol (DAAP) for MAS solid-state NMR of rotationally aligned membrane proteins in phospholipid bilayers.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2014Article
- SedNMR: a web tool for optimizing sedimentation of macromolecular solutes for SSNMR.Journal of biomolecular NMR · 2013Article
- Solid state NMR of proteins at high MAS frequencies: symmetry-based mixing and simultaneous acquisition of chemical shift correlation spectra.Journal of biomolecular NMR · 2012Article
- On the use of ultracentrifugal devices for sedimented solute NMR.Journal of biomolecular NMR · 2012Article
- Utilizing afterglow magnetization from cross-polarization magic-angle-spinning solid-state NMR spectroscopy to obtain simultaneous heteronuclear multidimensional spectra.The journal of physical chemistry. B · 2012Article
- Broadband excitation pulses for high-field solid-state nuclear magnetic resonance spectroscopy.Magnetic resonance in chemistry : MRC · 2012Article
Corrections and comments
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Authors and funding
4 authors.
Funding
Abstract
Three different techniques (adiabatic passage Hartman-Hahn cross-polarization, optimal control designed pulses, and EXPORT) are compared for transferring (15)N magnetization to (13)C in solid-state NMR experiments under magic-angle-spinning conditions. We demonstrate that, in comparison to adiabatic passage Hartman-Hahn cross-polarization, optimal control transfer pulses achieve similar or better transfer efficiencies for uniformly-(13)C,(15)N labeled samples and are generally superior for samples with non-uniform labeling schemes (such as 1,3- and 2-(13)C glycerol labeling). In addition, the optimal control pulses typically use substantially lower average RF field strengths and are more robust with respect to experimental variation and RF inhomogeneity. Consequently, they are better suited for demanding samples.
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