ArticleJournal of synchrotron radiation2011
Three-dimensional imaging of chemical phase transformations at the nanoscale with full-field transmission X-ray microscopy.
Article in Journal of synchrotron radiation, 2011. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 44 papers.
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Who cites it
44 citing papers in PubMed.
- Sub-20 nm Hard X-ray Spectromicroscopy Reveals Nanoscale Redox Heterogeneity in Ultrafine Particulates.ACS nano · 2026Article
- Data-driven deformation correction in X-ray spectro-tomography with implicit neural networks.Patterns (New York, N.Y.) · 2026Article
- Statistical White-Line Analysis in High-Throughput TXM-XANES for Chemical State Quantification.Photon science · 2026Article
- High-Speed X-Ray Imager 'Hayaka' and Its Application for Quick Imaging XAFS andSensors (Basel, Switzerland) · 2026Article
- pH variations enable guanine crystal formation within iridosomes.Nature chemical biology · 2026Article
- TXM-Pal: a companion software for advanced data processing in spectroscopic X-ray microscopy.Journal of synchrotron radiation · 2025Article
- Visualization of four-dimensional X-ray absorption fine structure data using a virtual reality system.Journal of synchrotron radiation · 2025Article
- Hyperspectral full-field quick-EXAFS imaging at the ROCK beamline for monitoring micrometre-sized heterogeneity of functional materials under process conditions.Journal of synchrotron radiation · 2024Article
- Nanoscale chemical imaging with structured X-ray illumination.Proceedings of the National Academy of Sciences of the United States of America · 2023Article
- X-ray Tomography Applied to Electrochemical Devices and Electrocatalysis.Chemical reviews · 2023Review
- Accurate real space iterative reconstruction (RESIRE) algorithm for tomography.Scientific reports · 2023Article
- Monochromatic computed tomography using laboratory-scale setup.Scientific reports · 2023Article
- Bridging nano- and microscale X-ray tomography for battery research by leveraging artificial intelligence.Nature nanotechnology · 2022Review
- Tracking dynamic structural changes in catalysis by rapid 2D-XANES microscopy.Journal of synchrotron radiation · 2021Article
- Sparse ab initio x-ray transmission spectrotomography for nanoscopic compositional analysis of functional materials.Science advances · 2021Article
- Depth-dependent valence stratification driven by oxygen redox in lithium-rich layered oxide.Nature communications · 2020Article
- Machine-learning-revealed statistics of the particle-carbon/binder detachment in lithium-ion battery cathodes.Nature communications · 2020Article
- Quantifying redox heterogeneity in single-crystalline LiCoOJournal of synchrotron radiation · 2020Article
- Charge distribution guided by grain crystallographic orientations in polycrystalline battery materials.Nature communications · 2020Article
- Translative lens-based full-field coherent X-ray imaging.Journal of synchrotron radiation · 2020Article
Corrections and comments
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Authors and funding
6 authors.
Funding
Abstract
The ability to probe morphology and phase distribution in complex systems at multiple length scales unravels the interplay of nano- and micrometer-scale factors at the origin of macroscopic behavior. While different electron- and X-ray-based imaging techniques can be combined with spectroscopy at high resolutions, owing to experimental time limitations the resulting fields of view are too small to be representative of a composite sample. Here a new X-ray imaging set-up is proposed, combining full-field transmission X-ray microscopy (TXM) with X-ray absorption near-edge structure (XANES) spectroscopy to follow two-dimensional and three-dimensional morphological and chemical changes in large volumes at high resolution (tens of nanometers). TXM XANES imaging offers chemical speciation at the nanoscale in thick samples (>20 µm) with minimal preparation requirements. Further, its high throughput allows the analysis of large areas (up to millimeters) in minutes to a few hours. Proof of concept is provided using battery electrodes, although its versatility will lead to impact in a number of diverse research fields.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.