Synthesis and characterization of some new tetraaldehyde and tetraketone derivatives and X-ray structure of 1,1'-(4,4'-(2-(1,3-bis(4-acetylphenoxy)propan-2-ylidene)propane-1,3-di-yl)bis(oxy)bis(4,1-phenylene))diethanone.

Mustafa Er, Reşat Ustabaş, Ufuk Çoruh, Kemal Sancak, Ezequiel Vázquez-López

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Article in International journal of molecular sciences, 2008. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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5 authors.

Mustafa ErDepartment of Chemistry Faculty of Arts and Sciences Karadeniz Teknik University, 61080-Trabzon, Turkey.

Reşat UstabaşDepartment of Middle Education, Educational Faculty, Ondokuz Mayıs University 55200-Atakum-Samsun, Turkey.

Ufuk ÇoruhDepartment of Computer Education and Instructional Technology, Educational Faculty, Ondokuz Mayıs University 55200-Atakum-Samsun, Turkey.

Kemal SancakDepartment of Chemistry Faculty of Arts and Sciences Karadeniz Teknik University, 61080-Trabzon, Turkey.

Ezequiel Vázquez-LópezDepartamento de Química Inorgánica, Facultade de Ciencias-Química, Universidade de Vigo, 36200-Vigo, Galicia, Spain.

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6 · The paper itself

Abstract

Tetraketone and tetraaldehyde derivatives 2a-d were synthesized via the reaction of ethene-1,1,2,2,-tetra-yl-tetramethylene tetrabromide (1) with hydroxyketone and aldehyde derivatives. The molecular structures were identified by IR, (1)H-NMR, (13)C-NMR and MS analysis. The crystal structure of the title compound 2a, C(38)H(36)O(8), is reported. Its crystal data are: monoclinic, space group P 2(1)/n with cell dimensions of a=9.0395(12) A, b=12.6114(17) A, c=13.8166(18) A, beta=95.875(3), V=1566.8(4) A(3), F.W.=620.67, rho(calc)=1.316 gcm(3) for Z=2, mu=0.092 mm(-1).

Indexed as

1,3-bis(4-Acetylphenoxy)propan-2-ylidenepropane1,3-di-ylbis(oxy)bis(4,1-phenylene))diethanonecrystal structurex-ray

Identifiers

PMID19325842

DOI10.3390/ijms9061000

PMCPMC2658780

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