ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2008
Biomolecular solid state NMR with magic-angle spinning at 25K.
Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2008. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 44 papers.
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Who cites it
44 citing papers in PubMed.
- Preserving integrity: innovative in vitro methods for extracellular matrix decellularization and collagen purification.Journal of biological engineering · 2026Article
- Time-resolved solid-state nuclear magnetic resonance studies of amyloid-β oligomer formation.Methods in enzymology · 2026Review
- Optimization ofJournal of magnetic resonance (San Diego, Calif. : 1997) · 2024Article
- Experimental Evidence for Millisecond-Timescale Structural Evolution Following the Microsecond-Timescale Folding of a Small Protein.Physical review letters · 2024Article
- Multi Electron Spin Cluster Enabled Dynamic Nuclear Polarization with Sulfonated BDPA.The journal of physical chemistry letters · 2023Article
- Diamond rotors.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2023Article
- Cryogenic-compatible spherical rotors and stators for magic angle spinning dynamic nuclear polarization.Magnetic resonance (Gottingen, Germany) · 2023Article
- Optical Fiber Temperature Sensors and Their Biomedical Applications.Sensors (Basel, Switzerland) · 2020Review
- Succinyl-DOTOPA: An effective triradical dopant for low-temperature dynamic nuclear polarization with high solubility in aqueous solvent mixtures at neutral pH.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2020Article
- Use of paramagnetic systems to speed-up NMR data acquisition and for structural and dynamic studies.Solid state nuclear magnetic resonance · 2019Review
- Tuning nuclear depolarization under MAS by electron TPhysical chemistry chemical physics : PCCP · 2018Article
- Pulsed Electron Decoupling and Strategies for Time Domain Dynamic Nuclear Polarization with Magic Angle Spinning.The journal of physical chemistry letters · 2018Article
- Low-temperature magnetic resonance imaging with 2.8 μm isotropic resolution.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2018Article
- Instrumentation for cryogenic magic angle spinning dynamic nuclear polarization using 90L of liquid nitrogen per day.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2017Article
- Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2016Article
- Pushing NMR sensitivity limits using dynamic nuclear polarization with closed-loop cryogenic helium sample spinning.Chemical science · 2015Article
- REDOR solid-state NMR as a probe of the membrane locations of membrane-associated peptides and proteins.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2015Article
- Magic angle spinning nuclear magnetic resonance characterization of voltage-dependent anion channel gating in two-dimensional lipid crystalline bilayers.Biochemistry · 2015Article
- Synthesis and evaluation of nitroxide-based oligoradicals for low-temperature dynamic nuclear polarization in solid state NMR.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2014Article
- Remote sensing of sample temperatures in nuclear magnetic resonance using photoluminescence of semiconductor quantum dots.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2014Article
Corrections and comments
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Authors and funding
2 authors.
Funding
Abstract
A magic-angle spinning (MAS) probe has been constructed which allows the sample to be cooled with helium, while the MAS bearing and drive gases are nitrogen. The sample can be cooled to 25K using roughly 3 L/h of liquid helium, while the 4-mm diameter rotor spins at 6.7 kHz with good stability (+/-5 Hz) for many hours. Proton decoupling fields up to at least 130 kHz can be applied. This helium-cooled MAS probe enables a variety of one-dimensional and two-dimensional NMR experiments on biomolecular solids and other materials at low temperatures, with signal-to-noise proportional to 1/T. We show examples of low-temperature (13)C NMR data for two biomolecular samples, namely the peptide Abeta(14-23) in the form of amyloid fibrils and the protein HP35 in frozen glycerol/water solution. Issues related to temperature calibration, spin-lattice relaxation at low temperatures, paramagnetic doping of frozen solutions, and (13)C MAS NMR linewidths are discussed.
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